掘进工作面瓦斯分级治理的技术研究

余吾煤业公司作为高瓦斯矿井,瓦斯吸附能力强,属低透气性难抽放煤层。矿井目前处于新旧采区重叠期、瓦斯含量双向变化重叠期,需要立足当前、分类施策,提升采掘效率。为进一步规范掘进工作面瓦斯治理,建立规范的瓦斯治理程序,介绍了掘进工作面瓦斯分级治理相关措施,确保掘进工作面安全生产有序进行。     

Evaluating the profile of myofibrillar proteins and its relationship with tenderness among five styles of dry-cured hams

In order to investigate the relationship between profile of myofibrillar proteins and tenderness among 2 kinds of Chinese hams (Jinhua and Xuanwei) and 3 kinds of European hams (Iberian, Serrano and Parma), shear force, myofibril fragmentation index (MFI), SDS-PAGE, carbonyls content and Raman spectroscopy were investigated. The shear force and salt content of Chinese hams were significantly higher than that of European hams, while moisture content was lower than that of European hams (p < 0.05). MFI values and SDS-PAGE profile revealed that the degradation of myofibrillar proteins in Chinese hams was lower than in European hams. In addition, Chinese hams showed significantly higher carbonyls content and β-sheet content compared with European hams, indicated that proteins aggregation intensively inhibited the degradation of myofibrillar proteins in Chinese hams. These results indicated that the higher shear force in Chinese style hams could be attributed to the lower moisture content and limited proteolysis.     

Acoustic damping flexible polyurethane foams: Effect of isocyanate index and water content on the soundproofing

High-efficiency sound absorbing flexible polyurethane foams (FPUFs) are manufactured using nonpolar polyester resin, methylene diphenyl diisocyanate, and other reagents by one-shot bulk polymerization. In this study, the impact of the isocyanate index (90, 100, and 110) and water content (2.5 and 5%) on the microphase separation and soundproofing behavior of FPUFs are examined using atomic force microscopy, Fourier transform infrared spectroscopy, optical microscope, and an impedance tube device. The results reveal that the increase of the isocyanate index and water content leads to the increase of the cell size, cell size distribution, open-cell content, cell wall roughness, and microphase separation. Also, maximum sound absorption coefficient (α) reaches to 0.98 and the average of α in the frequency range of 1500–4000 Hz increases from 0.7 to 0.87 by increasing the water content from 2.5 to 5% and isocyanate index from 90 to 110; therefore, acoustic damping performance enhances up to 26.24% due to the synergic effects of microphase separation on the viscose media formation, open-cell content, cell wall roughness, cell size, and cell size distribution. In conclusion, FPUFs with an optimal amount of microphase separation and drainage flow can be a promising candidate for sound insulating materials. © 2018 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2019 , 136, 47363.     

镁对非调质钢中组织及硫化物的影响

摘要：为了探究不同镁含量对非调质钢中组织和硫化物形态、尺寸、分布及成分的影响，采用蔡司金相显微镜、扫描电子显微镜、小样电解等方法，分析了经高温电阻炉冶炼不同镁添加量的49MnVS3非调质钢。结果表明，由于镁蒸气压较高，在实验室冶炼中大量挥发，导致钢中镁的实际平均收得率仅为310%；镁的质量分数为0～22×10-6时，随着镁的质量分数的增加，钢中硫化物形态由Ⅱ类逐渐向Ⅰ类、Ⅲ类转变；钢中硫化物尺寸增大，硫化物的分布均匀性得到显著改善；钢中复合夹杂物比例明显增加，但MnS的比例出现下降；形成了细小弥散的氧化物，增加了奥氏体形核质点，具有细化组织的趋势。     

一种提高油样中低含量石油磺酸盐分析效率的方法

为了准确分析油田化学驱采出液油样中石油磺酸盐的含量,介绍了一种在油样中加入不同极性溶剂组成的萃取体系的预处理技术,将石油磺酸盐萃取到水相,利用液相色谱仪对其进行检测的方法。取适量油样,依次加入正己烷、二氯甲烷、无水乙醇和蒸馏水,振荡均匀后静置分层,取下层水相溶液进行色谱分析。色谱柱为阴离子交换柱,流动相为甲醇/水和甲醇/盐水(含0.2 mol/L乙酸和0.2 mol/L乙酸铵),梯度洗脱。实验结果表明,该预处理技术联合液相色谱法检测技术分析效率较高,加标回收率高于90%,液相色谱最小定量限10 mg/L,线性范围10～2000 mg/L。该方法可对油样中低含量的石油磺酸盐进行快速定量分析。     

用气相色谱法检测顺酐生产中间物料组分

顺酐在常温下是固体,要制备成溶液才能进行气相色谱分析,所以溶剂的选择极为重要。为此,选用了稳定性好、沸点较高的乙腈作为溶剂,利用超声溶解,对生产中粗酐样品进行采样分析,并建立了气相色谱法测定顺酐中杂质含量的分析方法,可有效指导顺酐生产过程中的杂质组分分离,适用于顺酐生产的现场工艺控制。     

一种基于LTCC基板的数字光收发模块设计

首先介绍低温共烧陶瓷(LTCC)技术和数字光收发模块,阐述LTCC的技术特点、工艺流程以及它相较于传统PCB电路基板的优势,解释了数字光收发模块的通信原理和工作方式;其次,提出了一种基于LTCC电路基板的数字光收发模块的设计方案,详细介绍了该光模块的主要构成和实现方法,包括电路设计和关键器件的比较和选取;最后,通过对该方案所述的数字光收发模块的样件进行关键指标和性能测试,验证了该设计方案的可行性。     

A comparative study of 3E (energy,exergy, and economy) analysis of various solar stills

In this paper, an experimental study of the conventional solar still (CSS), the conventional solar still with glass cooling (CSSGC), the conventional solar still with basin heating (CSSBH), and the conventional solar still with glass cooling and basin heating (CSSGCBH) was carried out on the basis of the distilled water production, the energy efficiency (EnE), the exergy efficiency (ExE), and economic analysis. The CSSGC and CSSBH contain Peltier modules for cooling the glass and heating the basin. The evaporative heat transfer coefficient for all the experimental stills was calculated. The values of daily distilled water production from the CSSGCBH, CSSBH, CSSGC, and CSS were 4.56, 3.79, 2.49, and 1.89 kg/m², respectively. The daily distilled yield of the CSSBH and CSSGCBH were increased by 58.55% and 50.13%, respectively, as compared with the CSS. Moreover, the daily EnE and ExE of the CSSGCBH were 27.03% and 3.5%, respectively, whereas the EnE and ExE of the CSS were 10.88% and 1.3%, respectively. Furthermore, the cost of distilled water production was found to be 0.26, 0.35, 0.53, and 0.64 $/day for the CSS, CSSGC, CSSBH, and CSSGCBH, respectively, if the selling price of the distilled water was Rs10.     

Prediction of the water content of biodiesel using ANN-MLP: An environmental application

Fuel quality, especially biodiesel, is highly dependent on its water content, and the major sources of water in the fuel relate to the transportation, production, and storage processes. In this present contribution, the multilayer perceptron artificial neural network (MLP-ANN) was applied to predict the water content of biodiesel and diesel blend in terms of temperature and composition. The proposed algorithm was trained and tested by utilizing 400 experimental data points which were extracted from the literature. Based on the results, the MLP-ANN model has great ability to estimate the water content of biodiesel and diesel blend. The R-squared (R²), root mean square error, average absolute relative deviation, and a?bsolute deviation parameters for the total data set are obtained, respectively, as 0.99784, 123919.1172, 3.3632, and 1.17%, which indicate the effective performance suggested by ANN. As the computational study is cheaper and easier than the experimental study, the developed software could be considered as an alternative for laboratory study, and the environmental effect of biodiesel and produced undesired product after biodiesel combustion which is directly related to the water content of biodiesel is estimable with the information released in this study.     

基于加权法的砾类土含水率检测

砾类土在工程建设中有着广泛的应用,其含水率是一项非常重要的指标,但现有测试方法耗时较长。以砂砾石料的砾类土为试验对象,基于加权法思想,将饱和面干含水率替代法和虚拟比重法进行结合,开展砾类土含水率快速检测方法的研究,并对现有的饱和面干含水率测定操作进行一定的改进和优化。采用多种数学方法(绝对误差、均方偏差平方和,相关曲线的相关系数和F显著性检验分析法)对加权法和烘干法的结果进行对比分析。通过试验统计数据分析,证实加权法与烘干法的测定结果基本一致。该分析结果为现场土料含水率快速测定提供了一种新的思路和手段。